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KMID : 1059519950390100799
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Journal of the Korean Chemical Society
1995 Volume.39 No. 10 p.799 ~ p.805
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Preparation of Silane Dendrimer (Ⅱ)
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Kim Chung-Kyun
Park Eun-Mi
Kang Eun-Ju
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Abstract
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Silane dendrimer with 96 allylic end groups has been synthesized in excellent yield using repetitive alkenylation-hydrosilylation cycles. Each of the two steps provided the products in almost quantitative yields. After a simple chromotograpic purification (silica gel, chloroform), pure dendrimers were obtained and their purity was checked with 1H, 13C NMR spectroscopic method and elemental analysis.
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